Palmitoyl chloride → N-methyl-N-(2-palmitoyloxyethyl)benzamide

HRID 328441

Reaktionsgleichung

Reaktionsgleichung von HRID 328441
[CH3:1][N:2]([CH2:11][CH2:12][OH:13])[C:3](=[O:10])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[C:14](Cl)(=[O:30])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]>>[CH3:1][N:2]([CH2:11][CH2:12][O:13][C:14](=[O:30])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[C:3](=[O:10])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

Komponenten

3

Edukt 2

HCID 8206Palmitoyl chlorideHCID 4047264N-(2-hydroxyethyl)-N-methylbenzamide

Produkt 1

HCID 21441878N-methyl-N-(2-palmitoyloxyethyl)benzamide

Versuchsvorschrift

N-methyl-N-(2-palmitoyloxyethyl)benzamide was prepared by the procedure of example 1 from 18 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)benzamide and 26 gms. (0.1 mole) of palmitoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Aufarbeitung

  1. customN-methyl-N-(2-palmitoyloxyethyl)benzamide was prepared by the procedure of example 1 from 18 gms

Quellen und Nachweise

ORD-Eintrag
ord-a22d8476e6334d6093f69be5744eccf3
Quelldatensatz
uspto-grants-1977_04
Patentnummer
US04017522

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