Chloride → Magnesium Glycinate

HRID 328559

Reaktionsgleichung

Reaktionsgleichung von HRID 328559
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].C(=O)([O-])[O-].[Mg+2:10].[Cl-].Cl[O-].[Al+3].Cl[O-].Cl[O-]>O>[NH2:1][CH2:2][C:3]([O-:5])=[O:4].[Mg+2:10].[NH2:1][CH2:2][C:3]([O-:5])=[O:4]

Komponenten

6

Edukt 4

HCID 312ChlorideHCID 750GlycineHCID 11029Magnesium CarbonateHCID 22096649Aluminum chlorhydroxide

Produkt 1

HCID 84645Magnesium Glycinate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Reaktionsbedingungen

Temperatur
75 °C

Versuchsvorschrift

Magnesium glycinate was prepared by reacting 4 grams of glycine with 2.5 grams of basic magnesium carbonate (26.3% Mg) in 30 grams of water while agitating at 75° C. for one half hour. The cooled mixture was then added to 77 grams of zirconyl chloride (13.6% Zr) with stirring. To the above solution 100 grams of 50% aluminum chlorhydroxide (12.5% Al) was added with agitation. The mixture was heated at 85° C. for 20 minutes. The product was then evaporated at 53° C. under a vacuum of 200 mm of Hg and contained 15.8% Al, 13.6% Mg. 5.3% glycine and 22.1% Cl.

Aufarbeitung

  1. stirringwith stirring
  2. temperatureThe mixture was heated at 85° C. for 20 minutes
  3. customThe product was then evaporated at 53° C. under a vacuum of 200 mm of Hg

Quellen und Nachweise

ORD-Eintrag
ord-f3633a8a53cf4448a4418701373d167d
Quelldatensatz
uspto-grants-1977_04
Patentnummer
US04017599

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