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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 330530Erstellt: 25. Oktober 2026

Ammonia → HCID 54387914, Verbindung

https://huagongshe.com/reaction/330530

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAmmoniaHCID 222—
EduktEthanolHCID 702—
Edukt4-ChlorobenzalacetoneHCID 98183—
EduktRhodanineHCID 1201546—
ProduktHCID 54387914HCID 54387914—

Reaktionsschritte

A mixture of 1.33 g (0.01 mol) of rhodanine, 1.80 g (0.01 mol) of 4-chlorobenzalacetone, 20 ml of ethanol and 2 ml of aqueous ammonia was heated under reflux for 4 hours. After cooling, the precipitated crystals were recovered by filtration and washed with methanol to give 0.52 g of the desired 5-(α-methyl-4-chlorocinnamylidene)-4-oxo-2-thioxothiazolidine.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04897406
Quelldatensatzuspto-grants-1990_01
ORD IDord-cca7abc450654ffc956a09767c423888
Quellennotizuspto-grants-1990_01