4-Iodoaniline → 1-(4-Iodophenyl)-3-(4-sulfamoylphenyl)thiourea
Reaktionsgleichung
[N:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10]([NH2:13])(=[O:12])=[O:11])=[CH:6][CH:5]=1)=[C:2]=[S:3].[I:14][C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1>>[I:14][C:15]1[CH:21]=[CH:20][C:18]([NH:19][C:2](=[S:3])[NH:1][C:4]2[CH:5]=[CH:6][C:7]([S:10]([NH2:13])(=[O:11])=[O:12])=[CH:8][CH:9]=2)=[CH:17][CH:16]=1Komponenten
3
Versuchsvorschrift
The subject compound was prepared utilizing the procedure described above from 4-isothiocyanatobenzenesulfonamide and 4-iodoaniline. 1H NMR (400 MHz, DMSO-d6) δ 10.13 (s, 1H), 10.08 (s, 1H), 7.76-7.65 (m, 6H), 7.32 (d, J=8.8 Hz, 2H), 7.29 (bs, 2H); (M+H)+ (434).
Aufarbeitung
- customThe subject compound was prepared
Quellen und Nachweise
- ORD-Eintrag
- ord-122ac026f28e4c5180f646acdcc0f25f
- Quelldatensatz
- uspto-grants-2014_11