2-Hydroxyethyl acrylate → 2-(((3-(Methylsulfanyl)phenyl)carbamoyl)oxy)ethyl prop-2-enoate

HRID 336080

Reaktionsgleichung

Reaktionsgleichung von HRID 336080
C(C1C=C(C)C=C(C(C)(C)C)C=1O)(C)(C)C.CN(CCCN1CN(CCCN(C)C)CN(CCCN(C)C)C1)C.[CH3:41][S:42][C:43]1[CH:44]=[C:45]([N:49]=[C:50]=[O:51])[CH:46]=[CH:47][CH:48]=1.[C:52]([O:56][CH2:57][CH2:58][OH:59])(=[O:55])[CH:53]=[CH2:54].[N-]=C=O>>[C:52]([O:56][CH2:57][CH2:58][O:59][C:50](=[O:51])[NH:49][C:45]1[CH:46]=[CH:47][CH:48]=[C:43]([S:42][CH3:41])[CH:44]=1)(=[O:55])[CH:53]=[CH2:54]

Komponenten

6

Edukt 5

HCID 131652-Hydroxyethyl acrylateHCID 314042,6-Di-tert-butyl-4-methylphenolHCID 85160N,N',N''-Tris(3-dimethylaminopropyl)hexahydro-S-triazineHCID 105034IsocyanateHCID 1414183-(Methylthio)phenyl isocyanate

Produkt 1

HCID 592732622-(((3-(Methylsulfanyl)phenyl)carbamoyl)oxy)ethyl prop-2-enoate

Reaktionsbedingungen

Temperatur
60 °C

Versuchsvorschrift

0.02 g of 2,6-di-tert-butyl-4-methylphenol, 0.01 g of Desmorapid® Z, 11.7 g of 3-(methylthio)phenyl isocyanate were initially introduced and initially introduced into a 100 ml round-bottomed flask and heated to 60° C. Thereafter, 8.2 g of 2-hydroxyethyl acrylate were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Cooling was then effected. The product was obtained as a light yellow liquid. nD20:1.626.

Aufarbeitung

  1. additioninitially introduced into a 100 ml round-bottomed flask
  2. temperatureCooling
  3. customThe product was obtained as a light yellow liquid

Quellen und Nachweise

ORD-Eintrag
ord-07b85c56bd1d447aa6d3d4b972c1e8b6
Quelldatensatz
uspto-grants-2014_11
Patentnummer
US08889321B2

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