N-ethyl-3-methylaniline → Propanamide, N-ethyl-N-(3-methylphenyl)-

HRID 341744

Reaktionsgleichung

Reaktionsgleichung von HRID 341744
[CH2:1]([NH:3][C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[CH:5]=1)[CH3:2].[C:11](Cl)(=[O:14])[CH2:12][CH3:13]>>[CH2:1]([N:3]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[CH:5]=1)[C:11](=[O:14])[CH2:12][CH3:13])[CH3:2]

Komponenten

3

Edukt 2

HCID 7603N-ethyl-3-methylanilineHCID 62324Propionyl chloride

Produkt 1

HCID 44150680Propanamide, N-ethyl-N-(3-methylphenyl)-

Versuchsvorschrift

N-Ethyl-N-(3-methylphenyl)propionamide was prepared on a laboratory scale by acylation of N-ethyl-m-toluidine with propionyl chloride. The reaction was carried out in a 5 litre 3 necked round bottomed flask equipped with a mechanical stirrer, a thermometer (0°-250° C.), an addition vessel and a condenser.

Aufarbeitung

  1. customequipped with a mechanical stirrer
  2. customa thermometer (0°-250° C.), an addition vessel and a condenser

Quellen und Nachweise

ORD-Eintrag
ord-b8e167a762884ac4981728f815e679c1
Quelldatensatz
uspto-grants-1999_01
Patentnummer
US05856295

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