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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 342346Erstellt: 25. Oktober 2026

Ethanol → HCID 178447967, Verbindung

https://huagongshe.com/reaction/342346

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanolHCID 702—
EduktTolueneHCID 1140—
EduktHCID 178447942HCID 178447942—
KatalysatorPalladiumHCID 23938—
LösungsmittelHCID 178418361HCID 178418361—
ProduktHCID 178447967HCID 17844796763,2%

Reaktionsschritte

To a liquid mixture comprising 250 ml of ethanol and 250 ml of toluene was dissolved 92 g of the (4-(2-(trans-4-n-propylcyclohexyl)ethyl)cyclohexene-1-yl)benzene mentioned above, 5 g of palladium/carbon (5%) was added as catalyst thereto, and they were subjected to a catalytic reduction in hydrogen gas atmosphere. After finishing of the reaction, the catalyst was filtered off and the solvent was distilled off under a reduced pressure to obtain a yellow oily product. This product was recrystallized from ethanol to obtain 58.5 g of (trans-4-(2-(trans-4-n-propylcyclohexyl)ethyl)cyclohexyl)benzene.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05858275
Quelldatensatzuspto-grants-1999_01
ORD IDord-e2e2f4eab272414ebdf8b504cd6d8980
Quellennotizuspto-grants-1999_01