Methyl p-toluenesulfonate → HCID 86745141, Verbindung

HRID 345197Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 345197
[CH3:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[CH3:12][O:13][S:14]([C:17]1[CH:22]=[CH:21][C:20]([CH3:23])=[CH:19][CH:18]=1)(=[O:16])=[O:15]>>[CH3:12][N+:3]1[C:4]2[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=2)[CH:10]=[CH:11][C:2]=1[CH3:1].[CH3:23][C:20]1[CH:21]=[CH:22][C:17]([S:14]([OH:16])(=[O:15])=[O:13])=[CH:18][CH:19]=1

Komponenten

3

Edukt 2

HCID 6645Methyl p-toluenesulfonateHCID 70602-Methylquinoline

Produkt 1

HCID 86745141HCID 86745141, Verbindung

Versuchsvorschrift

2-Methyl-quinoline (71.5 pbw) and methyl-p-toluenesulfonate (102.3 pbw) are heated for about 10 minutes at 100° C. An exothermic reaction sets in, in which the mixture is heated to 180.C. After another 10 minutes the mixture is poured onto acetone, filtered with suction, washed with acetone and dried.

Aufarbeitung

  1. customAn exothermic reaction sets in, in which the mixture
  2. additionAfter another 10 minutes the mixture is poured onto acetone
  3. filtrationfiltered with suction
  4. washwashed with acetone
  5. customdried

Quellen und Nachweise

ORD-Eintrag
ord-d610caabd6674847a09a87c6df6e813e
Quelldatensatz
uspto-grants-1991_10
Patentnummer
US05055579

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