HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyanuric chloride → 2,4-Dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyanuric chloride | HCID 7954 | — |
| Edukt | 2,2,6,6-Tetramethyl-4-piperidyl benzoate | HCID 579967 | — |
| Lösungsmittel | O-Xylene | HCID 7237 | — |
| Produkt | 2,4-Dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine | HCID 19991752 | — |
Reaktionsschritte
46.1 g of cyanuric chloride and 136.0 g of 2,2,6,6-tetramethyl-4-benzoyloxypiperidine are reacted in 300 ml of xylene as described in Example 1 and worked up. After recrystallization from isopropanol, 2,4-dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine are obtained as colorless crystals having a melting point of 145°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05059689 |
| Quelldatensatz | uspto-grants-1991_10 |
| ORD ID | ord-9ec55a07da2b40dba42ea0dc185e7fc7 |
| Quellennotiz | uspto-grants-1991_10 |