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HRID345982

反应详情

EQUATION

反应方程式

HRID 345982 的结构方程式

REACTANTS

反应物

2
结构：Clc1nc(Cl)nc(Cl)n1
HCID7954

2,4,6-Trichloro-s-triazine

C3Cl3N3

结构：CC1(C)CC(OC(=O)c2ccccc2)CC(C)(C)N1
HCID579967

2,2,6,6-tetramethyl-4-piperidyl benzoate

C16H23NO2

PRODUCTS

生成物

1
结构：CC1(C)CC(OC(=O)c2ccccc2)CC(C)(C)N1c1nc(Cl)nc(Cl)n1
HCID19991752

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1C
溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

46.1 g of cyanuric chloride and 136.0 g of 2,2,6,6-tetramethyl-4-benzoyloxypiperidine are reacted in 300 ml of xylene as described in Example 1 and worked up. After recrystallization from isopropanol, 2,4-dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine are obtained as colorless crystals having a melting point of 145°.

WORKUP

后处理

  1. customAfter recrystallization from isopropanol, 2,4-dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine
  2. customare obtained as colorless crystals