HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid | HCID 13654696 | — |
| Produkt | 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride | HCID 13654698 | — |
Reaktionsschritte
The 1,2,2-trichloro-2,2-dimethylcyclopropanecarboxylic acid (3.0 g) synthesized in Example k and thionyl chloride (1.0 ml) were mixed, and reacted at 60° C. The reaction mixture was distilled under reduced pressure to give the desired 1,2,2-trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride (2.8 g) represented by the following formula. ##STR26##
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05061731 |
| Quelldatensatz | uspto-grants-1991_10 |
| ORD ID | ord-1c052737bb0341df8b9d2564b4ef283f |
| Quellennotiz | uspto-grants-1991_10 |