Ammonia → Benzenesulfinamide

HRID 358746

Reaktionsgleichung

Reaktionsgleichung von HRID 358746
[C:1]1([S:7](Cl)=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH3:10]>CCOCC>[C:1]1([S:7]([NH2:10])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Komponenten

4

Edukt 2

HCID 222AmmoniaHCID 4190003Benzenesulfinyl chloride

Produkt 1

HCID 11286519BenzenesulfinamideAusbeute 17 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 3283Diethyl EtherLösungsmittel

Versuchsvorschrift

Benzenesulphinamide was prepared by reacting benzenesulphinyl chloride with ammonia in ether initially at -78° C. and finally at ambient temperature and was isolated in 17% yield as a solid, m.p. 112°-115° C.

Aufarbeitung

  1. custominitially at -78° C.
  2. customfinally at ambient temperature and was isolated in 17% yield as a solid, m.p. 112°-115° C.

Quellen und Nachweise

ORD-Eintrag
ord-61f89b91a1154459a9933bf9d6056d4e
Quelldatensatz
uspto-grants-1991_03
Patentnummer
US04997844

Verknüpfte Notizen

Wird geladen…