Allylamine → 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]
Reaktionsgleichung
[N:1]([C:10]([CH3:16])([CH3:15])[C:11]([O:13]C)=O)=[N:2][C:3]([CH3:9])([CH3:8])[C:4]([O:6]C)=O.[CH2:17]([NH2:20])[CH:18]=[CH2:19]>CO>[N:2]([C:3]([CH3:8])([CH3:9])[C:4]([NH:20][CH2:17][CH:18]=[CH2:19])=[O:6])=[N:1][C:10]([CH3:16])([CH3:15])[C:11]([NH:20][CH2:17][CH:18]=[CH2:19])=[O:13]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Dimethyl 2,2'-azobis(2-methylpropionate) in an amount of 41.9 g, 48 ml of methanol, and 43 g of a 28% CH3ONa methanol solution were mixed and stirred for dissolution, followed by dropwise addition of 25 g of allylamine to react at 19° to 21° C. for 20 hours.
Aufarbeitung
- customto react at 19° to 21° C. for 20 hours
Quellen und Nachweise
- ORD-Eintrag
- ord-cbc849f2079f4b2e89bfcd0e603da8a8
- Quelldatensatz
- uspto-grants-1991_03
- Patentnummer
- US05001228
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