HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl piperazin-1-ylacetate → N-4-cyanobenzoyl-beta-phenyl-alpha,alpha-dimethyl-beta-alanyl-4-piperazineacetic acid benzyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl piperazin-1-ylacetate | HCID 18423308 | — |
| Edukt | N-4-cyanobenzoyl-beta-phenyl-alpha,alpha-dimethyl-beta-alanine | HCID 70199446 | — |
| Produkt | N-4-cyanobenzoyl-beta-phenyl-alpha,alpha-dimethyl-beta-alanyl-4-piperazineacetic acid benzyl ester | HCID 86753675 | 71,9% |
Reaktionsschritte
The same procedure as in Example 2-(6-2) was performed with N-4-cyanobenzoyl-β-phenyl-α,α-dimethyl-β-alanine (0.4 g, 1.24 mmol) and piperazineacetic acid benzyl ester (0.87 g, 3.72 mmol) to yield an oil of N-4-cyanobenzoyl-β-phenyl-α,α-dimethyl-β-alanyl-4-piperazineacetic acid benzyl ester (0.48 g, 70.0%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05866592 |
| Quelldatensatz | uspto-grants-1999_02 |
| ORD ID | ord-9cc90c3a9f09425c8baf43a68fd29469 |
| Quellennotiz | uspto-grants-1999_02 |