Methyl chloroacetate → 2-(4-Tert-butylphenoxy)acetic acid
Reaktionsgleichung
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].C[O:13][C:14](=[O:17])[CH2:15]Cl>>[C:1]([C:5]1[CH:6]=[CH:7][C:8]([O:11][CH2:15][C:14]([OH:17])=[O:13])=[CH:9][CH:10]=1)([CH3:4])([CH3:2])[CH3:3]Komponenten
3
Versuchsvorschrift
94% pure acid (melting point 93° to 95° C., 1.4% of residual phenol) was prepared in an analogous manner in a yield of 93.8% of theory from 4-tert-butylphenol and methylchloroacetate.
Quellen und Nachweise
- ORD-Eintrag
- ord-8e8f2143fb604e7eae47ec6f07c853c4
- Quelldatensatz
- uspto-grants-1999_02
- Patentnummer
- US05869735
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