Hydrate lead acetate → Lead diacetate
Reaktionsgleichung
[C:1]([O-:4])(=[O:3])[CH3:2].[Pb+2:5].O.[C:7]([O-:10])(=[O:9])[CH3:8]>CCCCOCCO>[C:1]([O-:4])(=[O:3])[CH3:2].[Pb+2:5].[C:7]([O-:10])(=[O:9])[CH3:8]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The hydrate lead acetate is dissolved in butoxyethanol (BuEtOH) (1) at 60° C. The resulting solution is kept at this temperature for two hours, and is cooled down slowly (2) to thereby form a precipitate of dehydrated lead acetate. The precipitation yield can be promoted by further cooling down the vessel containing said solution in an ice bath.
Quellen und Nachweise
- ORD-Eintrag
- ord-d2912ed95edd4b108b23c3a7feb1bdf4
- Quelldatensatz
- uspto-grants-2001_10
- Patentnummer
- US06300144B1
Notizen zur Reaktion
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