2-Amino-2-methyl-1-propanol → HCID 499734, Verbindung
Reaktionsgleichung
[CH2:1]([NH:3][C:4]1[C:5]([N:10]2[CH2:15][CH2:14][N:13]([C:16]([C:18]3[CH:26]=[CH:25][C:21]([C:22](O)=[O:23])=[CH:20][N:19]=3)=[O:17])[CH2:12][CH2:11]2)=[N:6][CH:7]=[CH:8][CH:9]=1)[CH3:2].[NH2:27][C:28]([CH3:32])([CH3:31])[CH2:29][OH:30]>>[CH3:31][C:28]([NH:27][C:22]([C:21]1[CH:25]=[CH:26][C:18]([C:16]([N:13]2[CH2:14][CH2:15][N:10]([C:5]3[C:4]([NH:3][CH2:1][CH3:2])=[CH:9][CH:8]=[CH:7][N:6]=3)[CH2:11][CH2:12]2)=[O:17])=[N:19][CH:20]=1)=[O:23])([CH3:32])[CH2:29][OH:30]Komponenten
3
Versuchsvorschrift
By the same procedure as described in the example 1, synthesis was carried out starting with 6-[1-[3-(ethylamino)-2-pyridyl]piperazin-4-yl-carbonyl]nicotinic acid and using 2-amino-2-methyl-1-propanol. And then, the product was recrystallized to give a desired compound.
Aufarbeitung
- customBy the same procedure as described in the example 1, synthesis
- customAnd then, the product was recrystallized