N-methoxymethyl-N-methylpyrrolidinium chloride → N-methoxymethyl-N-methylpyrrolidinium hexafluorophosphate

HRID 383189Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 383189
[Cl-].[CH3:2][O:3][CH2:4][N+:5]1([CH3:10])[CH2:9][CH2:8][CH2:7][CH2:6]1.[F:11][P-:12]([F:17])([F:16])([F:15])([F:14])[F:13].[K+]>O>[F:11][P-:12]([F:17])([F:16])([F:15])([F:14])[F:13].[CH3:2][O:3][CH2:4][N+:5]1([CH3:10])[CH2:9][CH2:8][CH2:7][CH2:6]1

Komponenten

4

Edukt 2

HCID 23116042N-methoxymethyl-N-methylpyrrolidinium chlorideHCID 23688904Potassium hexafluorophosphate

Produkt 1

HCID 86610880N-methoxymethyl-N-methylpyrrolidinium hexafluorophosphate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

A 20.0 g quantity of N-methoxymethyl-N-methylpyrrolidinium chloride prepared in Example 10 was dissolved in 120 g of water, and 22.2 g of potassium hexafluorophosphate was added to the solution, whereupon a white solid separated out. The mixture was stirred for 30 minutes, and dichloromethane was thereafter added to the mixture for extraction. The organic layer was washed with 120 g of water six times and then dried, affording 25.1 g of a white solid as the desired product.

Aufarbeitung

  1. customseparated out
  2. additiondichloromethane was thereafter added to the mixture for extraction
  3. washThe organic layer was washed with 120 g of water six times
  4. customdried

Quellen und Nachweise

ORD-Eintrag
ord-d358d06cb88a4fa083a00347a5157da7
Quelldatensatz
uspto-grants-2013_02
Patentnummer
US08366956B2

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