HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → Morpholine-3-carboxylic acid amide hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | 1,4-Dioxane | HCID 31275 | — |
| Edukt | tert-Butyl 3-carbamoylmorpholine-4-carboxylate | HCID 21098189 | — |
| Produkt | Morpholine-3-carboxylic acid amide hydrochloride | HCID 67166308 | — |
Reaktionsschritte
1,1-Dimethylethyl 3-(aminocarbonyl)morpholine-4-carboxylate (0.48 g, 2.085 mmol) was taken up in 4 M HCl in dioxane (5 mL, 10.00 mmol) and maintained at room temperature overnight. The solvent was removed in vacuo to afford the title compound as a pale yellow solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08367706B2 |
| Quelldatensatz | uspto-grants-2013_02 |
| ORD ID | ord-11ae47b014e3454b84fe5e46e12c8be8 |
| Quellennotiz | uspto-grants-2013_02 |