Reaktionsgleichung
[CH2:1]([NH2:5])[CH2:2][CH2:3][CH3:4].[CH3:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[C:12]([O:15]CC)(=[O:14])C>>[CH2:1]([NH:5][C:12](=[O:14])[O:15][C:8]1[CH:7]=[CH:6][CH:11]=[CH:10][CH:9]=1)[CH2:2][CH2:3][CH3:4]Komponenten
4
Versuchsvorschrift
n-Butylamine (4.9 ml, 50 mmol) was used for the same reaction as in Production Example 310-1, and purification was performed by silica gel column chromatography (hexane:ethyl acetate=4:1) to obtain the title compound (8.11 g, 41.97 mmol, 71.97%) as a colorless oil.
Quellen und Nachweise
- ORD-Eintrag
- ord-d622430da6ac4852a075f4b60e9d89f9
- Quelldatensatz
- uspto-grants-2013_02
- Patentnummer
- US08372981B2
Verknüpfte Notizen
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