HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl mercaptan → 1-Benzylsulfanyl-3-bromo-2-trifluoromethyl-benzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl mercaptan | HCID 7509 | — |
| Edukt | 2-Bromo-6-fluorobenzotrifluoride | HCID 2773345 | — |
| Produkt | 1-Benzylsulfanyl-3-bromo-2-trifluoromethyl-benzene | HCID 67155259 | — |
Reaktionsschritte
Phenyl-methanethiol (4.g g, 37.0 mmol) was treated with commercially available 1-bromo-3-fluoro-2-trifluoromethyl-benzene (10.0 g, 41.1 mmol) in close analogy to the procedure described in step 5.3). The crude product (10.5 g) after workup was used as such in the next reaction step without purification by chromatography.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08378092B2 |
| Quelldatensatz | uspto-grants-2013_02 |
| ORD ID | ord-e82cb9c16d524ad382d59b2d011bdb18 |
| Quellennotiz | uspto-grants-2013_02 |