Octyltrichlorosilane → HCID 13977504, Verbindung

HRID 395241

Reaktionsgleichung

Reaktionsgleichung von HRID 395241
[C:1]([O-:4])(=[O:3])[CH3:2].[Na+].[CH2:6]([Si:14](Cl)(Cl)Cl)[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]>CCCCCCC>[CH2:6]([Si:14]([O:4][C:1](=[O:3])[CH3:2])([O:3][C:1](=[O:4])[CH3:2])[O:3][C:1](=[O:4])[CH3:2])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

Komponenten

4

Edukt 2

HCID 21354OctyltrichlorosilaneHCID 517045Sodium Acetate

Produkt 1

HCID 13977504HCID 13977504, VerbindungAusbeute 88 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8900HeptaneLösungsmittel

Versuchsvorschrift

In a 1-1 round-bottomed flask were placed first 55 g of anhydrous sodium acetate, and then 500 ml of anhydrous heptane. To the white suspension formed was added 50 g of octyltrichlorosilane. The reaction medium was left under stirring at ambient temperature for 2 h, and then filtered under argon to remove the precipitate. The filtrate was concentrated to eliminate the heptane, giving 54 g (88% yield) of octyltriacetoxysilane as a colorless oil.

Aufarbeitung

  1. customTo the white suspension formed
  2. waitThe reaction medium was left
  3. filtrationfiltered under argon
  4. customto remove the precipitate
  5. concentrationThe filtrate was concentrated

Quellen und Nachweise

ORD-Eintrag
ord-4ac068724ab44b20bce208aa01a6c954
Quelldatensatz
uspto-grants-2003_08
Patentnummer
US06605423B2

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