HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Jineol → 3,8-Dimethoxy quinoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Jineol | HCID 177338 | — |
| Edukt | Diazomethane diethylether | HCID 21186548 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3,8-Dimethoxy quinoline | HCID 10583798 | 80% |
Reaktionsschritte
Jineol of 4.5 mg was dissolved in 2 ml of ethanol, and diazomethane ether solution was slowly dropped to the solution. After the excess of diazomethane and solvent was removed by purging with nitrogen gas, the solution was purified by silicagel chromatography to give 4.2 mg of 3,8-dimethoxy quinoline with 80% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05824689 |
| Quelldatensatz | uspto-grants-1998_10 |
| ORD ID | ord-a3d35d944aca43608a8e9c356519b602 |
| Quellennotiz | uspto-grants-1998_10 |