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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 399742Erstellt: 26. Oktober 2026

Jineol → 3,8-Dimethoxy quinoline

https://huagongshe.com/reaction/399742

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktJineolHCID 177338—
EduktDiazomethane diethyletherHCID 21186548—
LösungsmittelEthanolHCID 702—
Produkt3,8-Dimethoxy quinolineHCID 1058379880%

Reaktionsschritte

Jineol of 4.5 mg was dissolved in 2 ml of ethanol, and diazomethane ether solution was slowly dropped to the solution. After the excess of diazomethane and solvent was removed by purging with nitrogen gas, the solution was purified by silicagel chromatography to give 4.2 mg of 3,8-dimethoxy quinoline with 80% yield.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05824689
Quelldatensatzuspto-grants-1998_10
ORD IDord-a3d35d944aca43608a8e9c356519b602
Quellennotizuspto-grants-1998_10