2-Fluoro-N-(2-methoxy-ethyl)-4-methylamino-5-nitro-benzamide → 5-Amino-2-fluoro-N-(2-methoxy-ethyl)-4-methylamino-benzamide
Reaktionsgleichung
[F:1][C:2]1[CH:14]=[C:13]([NH:15][CH3:16])[C:12]([N+:17]([O-])=O)=[CH:11][C:3]=1[C:4]([NH:6][CH2:7][CH2:8][O:9][CH3:10])=[O:5]>[Pd]>[NH2:17][C:12]1[C:13]([NH:15][CH3:16])=[CH:14][C:2]([F:1])=[C:3]([CH:11]=1)[C:4]([NH:6][CH2:7][CH2:8][O:9][CH3:10])=[O:5]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
5-Amino-2-fluoro-N-(2-methoxy-ethyl)-4-methylamino-benzamide (72 mg) was prepared by following General Procedure B starting from 2-fluoro-N-(2-methoxy-ethyl)-4-methylamino-5-nitro-benzamide and Pd/C (10% by weight, 10 mg). Th crude product was used in the next step without further purification.
Aufarbeitung
- customTh crude product was used in the next step without further purification