HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Anhydride → 1-Acetyl-7-methylindoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | 7-Methyl-2,3-dihydro-1H-indole | HCID 12377788 | — |
| Produkt | 1-Acetyl-7-methylindoline | HCID 14361366 | — |
Reaktionsschritte
A solution of 7-methylindoline (10.2 g) in acetic anhydride (25 ml) was refluxed for 30 min. After cooling, the reaction solution was poured into ice water (250 ml) and the resulting crystal was filtered by means of suction, heated and vacuum dried to yield the end product (11.7 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06559149B1 |
| Quelldatensatz | uspto-grants-2003_05 |
| ORD ID | ord-532146205184410b96c1b186bb23c4a5 |
| Quellennotiz | uspto-grants-2003_05 |