Sulfuric Acid → 5-Chlorohexanoic acid

HRID 411807

Reaktionsgleichung

[C:1]([OH:8])(=[O:7])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].S(=O)(=O)(O)O.[Cl:14]N(C(C)C)C(C)C>>[Cl:14][CH:5]([CH3:6])[CH2:4][CH2:3][CH2:2][C:1]([OH:8])=[O:7]

Komponenten

Edukt 3

HCID 1118Sulfuric Acid

HCID 8892Hexanoic Acid

HCID 32745N-Chloro-N,N-diisopropylamine

Produkt 1

HCID 185416685-Chlorohexanoic acid

Versuchsvorschrift

135 parts by mass of the caproic acid were added to 1,000 parts by mass of 84% sulfuric acid and an equivalent amount of N-chlorodiisopropylamine and were reacted for 5 hours at 25° C. to obtain 163 parts by mass of 5-chlorocaproic acid.

Quellen und Nachweise

ORD-Eintrag: ord-e00c1458200e40adb14489b39ada7486
Quelldatensatz: uspto-grants-2003_05
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06559275B2

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