Hydrochloric Acid → methyl 1H-tetrazol-1-ylacetate

HRID 419839Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 419839
[N:1]1([CH2:6][C:7]([OH:9])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1.Cl.O1CCOC[CH2:12]1>CO>[N:1]1([CH2:6][C:7]([O:9][CH3:12])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 312751,4-DioxaneHCID 5432071-Tetrazolylacetic acid

Produkt 1

HCID 3153776methyl 1H-tetrazol-1-ylacetate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

A mixture of tetrazol-1-yl acetic acid (5 g, 39 mmol) and 4M hydrochloric acid in dioxan (100 μL) in methanol (50 mL) was heated under reflux for 18 hours. The cooled mixture was evaporated under reduced pressure to provide the title compound.

Aufarbeitung

  1. temperaturewas heated
  2. temperatureunder reflux for 18 hours
  3. customThe cooled mixture was evaporated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-1f14cc65617e4ae1985a9137fda2cfc7
Quelldatensatz
uspto-grants-2012_01
Patentnummer
US08093400B2

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