Thiophenol → 1,3-Dimethyl-2,4-dioxo-6-(phenylthio)-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

HRID 42698

Reaktionsgleichung

Reaktionsgleichung von HRID 42698
Cl[C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[C:4](=[O:11])[C:3]=1[CH:12]=[O:13].[C:14]1([SH:20])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[CH3:8][N:7]1[C:2]([S:20][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[C:3]([CH:12]=[O:13])[C:4](=[O:11])[N:5]([CH3:10])[C:6]1=[O:9]

Komponenten

3

Edukt 2

HCID 7969ThiophenolHCID 3199716-Chloro-5-formyl-1,3-dimethyluracil

Produkt 1

HCID 866586861,3-Dimethyl-2,4-dioxo-6-(phenylthio)-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Versuchsvorschrift

The process described in Method D was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (1.50 g, 7.40 mmol) and benzenethiol were used to obtain the title compound.

Quellen und Nachweise

ORD-Eintrag
ord-d7f338fee3cd4f0ab01d9159128e14d9
Quelldatensatz
uspto-grants-2013_09
Patentnummer
US08536210B2

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