2,5-Dimethylbenzaldehyde → [5-(2,5-Dimethyl-phenyl)-imidazo[1,2-b][1,2,4]triazol-6-yl]-(1,1,3,3-tetramethyl-butyl)-amine

HRID 431233

Reaktionsgleichung

Reaktionsgleichung von HRID 431233
[NH2:1][C:2]1[N:6]=[CH:5][NH:4][N:3]=1.[CH3:7][C:8]([N+:15]#[C-:16])([CH3:14])[CH2:9][C:10]([CH3:13])([CH3:12])[CH3:11].[CH3:17][C:18]1[CH:25]=[CH:24][C:23]([CH3:26])=[CH:22][C:19]=1[CH:20]=O>Cl(O)(=O)(=O)=O>[CH3:17][C:18]1[CH:25]=[CH:24][C:23]([CH3:26])=[CH:22][C:19]=1[C:20]1[N:1]=[C:2]2[N:6]=[CH:5][NH:4][N:3]2[C:16]=1[NH:15][C:8]([CH3:14])([CH3:7])[CH2:9][C:10]([CH3:13])([CH3:12])[CH3:11]

Komponenten

5

Edukt 3

HCID 220152,5-DimethylbenzaldehydeHCID 267251,1,3,3-Tetramethylbutyl isocyanideHCID 178418311HCID 178418311, Verbindung

Produkt 1

HCID 22335552[5-(2,5-Dimethyl-phenyl)-imidazo[1,2-b][1,2,4]triazol-6-yl]-(1,1,3,3-tetramethyl-butyl)-amine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 24247Perchloric AcidLösungsmittel

Versuchsvorschrift

Compound 54 was prepared in accordance with the general synthesis instructions from 1.0 ml (0.1 mmol) 3-amino-1,2,4-triazole solution (0.1 M, MC), 0.575 ml (0.115 mmol) 1,1,3,3-tetramethylbutylisonitrile solution (0.2 M, MC), 0.500 ml (0.15 mmol) 2,5-dimethylbenzaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%).

Quellen und Nachweise

ORD-Eintrag
ord-187b8c0a3f59403394a9d6e9260423da
Quelldatensatz
uspto-grants-2003_12
Patentnummer
US06657064B2

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