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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 431418Erstellt: 26. Oktober 2026

Trimethylamine → 1,3-Dihydroxy-5-trimethylsiloxyadamantane

https://huagongshe.com/reaction/431418

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTrimethylamineHCID 1146—
EduktChlorotrimethylsilaneHCID 6397—
Edukt1,3,5-AdamantanetriolHCID 9899022—
LösungsmittelDichloromethaneHCID 6344—
Produkt1,3-Dihydroxy-5-trimethylsiloxyadamantaneHCID 21930710—

Reaktionsschritte

This 1,3,5-trihydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an equimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature. The reaction product was partitioned by high performance liquid chromatography to obtain 1,3-dihydroxy-5-trimethylsiloxyadamantane.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06660450B2
Quelldatensatzuspto-grants-2003_12
ORD IDord-609fd757932c4d9781e7d8b82ed4d6a3
Quellennotizuspto-grants-2003_12