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HRID431418

反应详情

EQUATION

反应方程式

HRID 431418 的结构方程式

REACTANTS

反应物

3
结构：CN(C)C
HCID1146

Trimethylamine

C3H9N

结构：C[Si](C)(C)Cl
HCID6397

Chlorotrimethylsilane

C3H9ClSi

结构：OC12CC3CC(O)(C1)CC(O)(C3)C2
HCID9899022

1,3,5-Adamantanetriol

C10H16O3

PRODUCTS

生成物

1
结构：C[Si](C)(C)OC12CC3CC(O)(CC(O)(C3)C1)C2
HCID21930710

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

This 1,3,5-trihydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an equimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature. The reaction product was partitioned by high performance liquid chromatography to obtain 1,3-dihydroxy-5-trimethylsiloxyadamantane.

WORKUP

后处理

  1. customReaction
  2. customwas carried out at room temperature
  3. customThe reaction product was partitioned by high performance liquid chromatography