Phenyl Salicylate → 2'-Ethyl-salicylanilide

HRID 433030

Reaktionsgleichung

Reaktionsgleichung von HRID 433030
[C:1]([O:10]C1C=CC=CC=1)(=O)[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[CH2:17]([C:19]1[CH:25]=[CH:24][CH:23]=[CH:22][C:20]=1[NH2:21])[CH3:18]>>[CH2:17]([C:19]1[CH:25]=[CH:24][CH:23]=[CH:22][C:20]=1[NH:21][C:1](=[O:10])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4])[CH3:18]

Komponenten

3

Edukt 2

HCID 8361Phenyl SalicylateHCID 113572-Ethylaniline

Produkt 1

HCID 187609142'-Ethyl-salicylanilide

Versuchsvorschrift

The 2′-ethyl-salicylanilide was prepared by condensing phenyl salicylate with 2-ethylaniline then purified as described in Example 2a. The ligand mixture was then prepared from 2′-ethyl-salicylanilide and 1,1′-bi-2-naphthol using the procedure described in Example 2a. 31P NMR (121.77 MHz): several peaks between 117.1-118.8 ppm.

Aufarbeitung

  1. customthen purified
  2. customThe ligand mixture was then prepared from 2′-ethyl-salicylanilide and 1,1′-bi-2-naphthol using the procedure

Quellen und Nachweise

ORD-Eintrag
ord-4bbf13c0bf514f11b9c4464537d267e6
Quelldatensatz
uspto-grants-2003_12
Patentnummer
US06664427B1

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