Sodium → D-glycero-D-gulo-heptonic acid

HRID 434492

Reaktionsgleichung

Reaktionsgleichung von HRID 434492
[Na].[CH2:2]([OH:16])[C@@H:3]([OH:15])[C@@H:4]([OH:14])[C@H:5]([OH:13])[C@@H:6]([OH:12])[C@@H:7]([OH:11])[C:8]([O-:10])=[O:9].[Na+]>O.O[Mo](O)(=O)=O>[CH2:2]([OH:16])[C@@H:3]([OH:15])[C@@H:4]([OH:14])[C@H:5]([OH:13])[C@@H:6]([OH:12])[C@@H:7]([OH:11])[C:8]([OH:10])=[O:9]

Komponenten

5

Edukt 2

HCID 5360545SodiumHCID 23664054Gluceptate Sodium

Produkt 1

HCID 25588D-glycero-D-gulo-heptonic acid

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 82208Molybdic acidKatalysatorHCID 962WaterLösungsmittel2×

Reaktionsbedingungen

Temperatur
25 °C

Versuchsvorschrift

The molybdenum ester of glucoheptonic acid was prepared as follows: Approximately 241 grams (1 mol) of the sodium salt of molybdic acid (sodium molybdenate) and 248 grams (1 mol) of sodium glucoheptonate were charged to an esterification vessel containing about 600 ml. of water as a solvent. With stirring, the temperature was maintained at about 25° C. for approximately 30 minutes. The mixture was thereafter diluted to a final volume of one liter with additional water.

Aufarbeitung

  1. additioncontaining about 600 ml

Quellen und Nachweise

ORD-Eintrag
ord-7d201175ba1b4101920c7c473c66295e
Quelldatensatz
uspto-grants-1983_08
Patentnummer
US04397812

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