Ammonium Hydroxide → 2-Amino-6-methoxypyrazine 4-oxide

HRID 441735Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 441735
Cl[C:2]1[CH:7]=[N+:6]([O-:8])[CH:5]=[C:4]([O:9][CH3:10])[N:3]=1.[OH-].[NH4+:12]>>[NH2:12][C:2]1[CH:7]=[N+:6]([O-:8])[CH:5]=[C:4]([O:9][CH3:10])[N:3]=1

Komponenten

3

Edukt 2

HCID 14923Ammonium HydroxideHCID 205289402-Chloro-6-methoxypyrazine 4-oxide

Produkt 1

HCID 205289822-Amino-6-methoxypyrazine 4-oxide

Versuchsvorschrift

2-Chloro-6-methoxypyrazine 4-oxide is treated with an excess of ammonium hydroxide in an autoclave at 150° C. for 14 hours. The reaction mixture is cooled and evaporated to dryness to give the crude product which may be used in the next step as is.

Aufarbeitung

  1. temperatureThe reaction mixture is cooled
  2. customevaporated to dryness

Quellen und Nachweise

ORD-Eintrag
ord-b4ba8aed85694781b34d4c8470541b07
Quelldatensatz
uspto-grants-1977_08
Patentnummer
US04042586

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