HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → Ethyl 3-bromo-4-methoxyphenylacetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | 3-Bromo-4-methoxyphenylacetic acid | HCID 136615 | — |
| Katalysator | Hydrochloric Acid | HCID 313 | — |
| Produkt | Ethyl 3-bromo-4-methoxyphenylacetate | HCID 57419861 | — |
Reaktionsschritte
A solution of 3-bromo-4-methoxyphenylacetic acid (4.1 g, 16.7 mmol) and concentrated hydrogen chloride (2 drops) in EtOH (100 mL) were stirred at 80° C. for 3 days. After cooling to room temperature, the mixture was concentrated to dryness to give the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08497381B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-40154bfaaa5f406ca5094da0897e0562 |
| Quellennotiz | uspto-grants-2013_07 |