1,4-Butanediol → Sulfamic acid, tetramethylene ester
Reaktionsgleichung
S(O[CH2:6][CH2:7][O:8][S:9](=[O:12])(=[O:11])[NH2:10])(=O)(=O)N.[CH2:13]([OH:18])[CH2:14]CCO>>[S:9]([O:18][CH2:13][CH2:14][CH2:6][CH2:7][O:8][S:9](=[O:11])(=[O:12])[NH2:10])(=[O:11])(=[O:8])[NH2:10]Komponenten
3
Versuchsvorschrift
1,4-Bis-O-sulfamyl-1,4-butanediol is prepared in the same manner as 1,2-bis-O-sulfamyl-1,2-ethanediol in Example 1 except that 1,4-butanediol (34.6 g., 0.385 mol.) is employed as the alkanediol.
Quellen und Nachweise
- ORD-Eintrag
- ord-30733bd823444943b27db5a6f25489d7
- Quelldatensatz
- uspto-grants-1977_12
- Patentnummer
- US04061663
Notizen zur Reaktion
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