HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 2-Chloro-4'-methyl-3'-sulfamoylacetophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Isopropanol | HCID 3776 | — |
| Edukt | 4'-Methyl-3'-sulfamoyl-diazoacetophenone | HCID 54047535 | — |
| Lösungsmittel | Diglyme | HCID 8150 | — |
| Produkt | 2-Chloro-4'-methyl-3'-sulfamoylacetophenone | HCID 13628783 | — |
Reaktionsschritte
10 g of 4'-methyl-3'-sulfamoyl-diazoacetophenone were reacted as prescribed in Example 66b) in diethylene glycol dimethyl ether with 37% HCl and worked up. Colorless crystals, melting point: 166° C (from isopropanol).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04061761 |
| Quelldatensatz | uspto-grants-1977_12 |
| ORD ID | ord-090ae4e346d942ee9c943031c6a5fdbd |
| Quellennotiz | uspto-grants-1977_12 |