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HRID461155

反应详情

EQUATION

反应方程式

HRID 461155 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)O
HCID3776

Isopropanol

C3H8O

结构：Cc1ccc(C(=O)C=[N+]=[N-])cc1S(N)(=O)=O
HCID54047535

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(C(=O)CCl)cc1S(N)(=O)=O
HCID13628783

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：COCCOCCOC
溶剂HCID8150

Diethylene glycol dimethyl ether

C6H14O3

PROCEDURE

实验过程

10 g of 4'-methyl-3'-sulfamoyl-diazoacetophenone were reacted as prescribed in Example 66b) in diethylene glycol dimethyl ether with 37% HCl and worked up. Colorless crystals, melting point: 166° C (from isopropanol).