Water → HCID 24708775, Verbindung

HRID 461519

Reaktionsgleichung

Reaktionsgleichung von HRID 461519
[OH:1][C:2]1[CH:12]=[CH:11][C:5]([CH2:6][CH2:7][C:8](=[O:10])[CH3:9])=[CH:4][CH:3]=1.[OH-].[K+].[CH2:15](Br)[CH:16]=[CH2:17].O>C(O)C>[CH2:17]([O:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][CH2:7][C:8](=[O:10])[CH3:9])=[CH:11][CH:12]=1)[CH:16]=[CH2:15]

Komponenten

6

Edukt 4

HCID 962WaterHCID 7841Allyl bromideHCID 14797Potassium HydroxideHCID 216484-(4'-Hydroxyphenyl)-2-butanone

Produkt 1

HCID 24708775HCID 24708775, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

p-Hydroxy benzylacetone (1.5 g.), KOH (6 g.) and allyl bromide (1.2 g.) were stirred in ethanol (50 ml) overnight. Water was added and the mixture extracted with ether, which was evaporated to give the compound (1.6 g.) as an oil purified by column chromatography.

Aufarbeitung

  1. extractionthe mixture extracted with ether, which
  2. customwas evaporated
  3. customto give the compound (1.6 g.) as an oil
  4. custompurified by column chromatography

Quellen und Nachweise

ORD-Eintrag
ord-67502816a83c4a06a3fe4d307df71c29
Quelldatensatz
uspto-grants-1977_12
Patentnummer
US04062978

Verknüpfte Notizen

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