Water → HCID 178511811, Verbindung
Reaktionsgleichung
[NH2:1][C@H:2]([C:9]([OH:11])=[O:10])[CH2:3][C:4]1[N:8]=[CH:7][NH:6][CH:5]=1.[OH:12][P:13]([F:16])([OH:15])=[O:14].O>CO.C(O)C>[P:13]([F:16])([OH:15])([OH:14])=[O:12].[NH2:1][C@H:2]([C:9]([OH:11])=[O:10])[CH2:3][C:4]1[N:8]=[CH:7][NH:6][CH:5]=1Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
L-histidine monofluorophosphate was prepared by combining 31 gm. of free-base L-histidine with 20 gm. of monofluorophosphoric acid in about 75 ml. of water. A clear syrup resulted. The syrup was poured into 750 ml. of a methanol-ethanol mixture. The precipitate (L-histidine monofluorophosphate) was collected and vacuum dried in a desiccator.
Aufarbeitung
- customA clear syrup resulted
- additionThe syrup was poured into 750 ml
- customThe precipitate (L-histidine monofluorophosphate) was collected
- customvacuum dried in a desiccator
Quellen und Nachweise
- ORD-Eintrag
- ord-17e90312b2714341854be25add764976
- Quelldatensatz
- uspto-grants-1977_12
- Patentnummer
- US04064138
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