HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 12783831, Verbindung → 2-[3-(N-benzyl-N-pyrid-2-ylamino)propylamino]-5-(5,6-dimethylpyrid-3-ylmethyl)pyrimid-4-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 12783831 | HCID 12783831 | — |
| Edukt | 2-[N-(3-aminopropyl)-N-benzylamino)pyridine | HCID 20150364 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | 2-[3-(N-benzyl-N-pyrid-2-ylamino)propylamino]-5-(5,6-dimethylpyrid-3-ylmethyl)pyrimid-4-one | HCID 20262889 | — |
Reaktionsschritte
2-[N-(3-aminopropyl)-N-benzylamino]pyridine (1 g) and 2-nitroamino-5-(5,6-dimethylpyrid-3-ylmethyl)pyrimid-4-one (0.94 g) were heated together under reflux in pyridine (5 ml) for 20 hrs. After stripping the resulting solid was recrystallized from ethanol/water to give 2-[3-(N-benzyl-N-pyrid-2-ylamino)propylamino]-5-(5,6-dimethylpyrid-3-ylmethyl)pyrimid-4-one 0.75 H2O, 0.61 g (38%) m.p. 95°-99° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04547506 |
| Quelldatensatz | uspto-grants-1985_10 |
| ORD ID | ord-4974f2a97c3d4c14a9d1f882eb801b2b |
| Quellennotiz | uspto-grants-1985_10 |