Sodium 4-styrenesulfonate → 1-(p-Methacryloxyphenyl)-2,6-dimethyl-3-nonylpyridinium p-styrene sulfonate

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Reaktionsgleichung

[Cl-].[C:2]([O:7][C:8]1[CH:13]=[CH:12][C:11]([N+:14]2[C:19]([CH3:20])=[CH:18][CH:17]=[C:16]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[C:15]=2[CH3:30])=[CH:10][CH:9]=1)(=[O:6])[C:3]([CH3:5])=[CH2:4].[CH2:31]=[CH:32][C:33]1[CH:38]=[CH:37][C:36]([S:39]([O-:42])(=[O:41])=[O:40])=[CH:35][CH:34]=1.[Na+]>ClCCCl>[CH2:31]=[CH:32][C:33]1[CH:34]=[CH:35][C:36]([S:39]([O-:42])(=[O:41])=[O:40])=[CH:37][CH:38]=1.[C:2]([O:7][C:8]1[CH:13]=[CH:12][C:11]([N+:14]2[C:19]([CH3:20])=[CH:18][CH:17]=[C:16]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[C:15]=2[CH3:30])=[CH:10][CH:9]=1)(=[O:6])[C:3]([CH3:5])=[CH2:4]

Komponenten

Reaktionsbedingungen

Temperatur: 45 °C

Versuchsvorschrift

To a 20 percent w/v 1,2-dichloroethane solution of 1-(p-methacryloxyphenyl)-2,6-dimethyl-3-nonylpyridinium chloride is added 150 g of sodium p-styrene sulfonate. The slurry is heated to 45° C. and stirred for 4 hours. The solids are separated from the supernatant liquid and the 1,2-dichloroethane is removed to give an oil of 1-(p-methacryloxyphenyl)-2,6-dimethyl-3-nonylpyridinium p-styrene sulfonate.

Aufarbeitung

customThe solids are separated from the supernatant liquid
customthe 1,2-dichloroethane is removed

Quellen und Nachweise

ORD-Eintrag: ord-cd8c9ae497e04588b70141c5c3d40037
Quelldatensatz: uspto-grants-1992_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05159035

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