Phenol → 4-Hydroxyphenylglycine
Reaktionsgleichung
[C:1]([O-:5])(=[O:4])[CH:2]=O.[NH4+:6].C([O-])(=O)C.[NH4+].[C:12]1([OH:18])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>O>[CH:14]1[C:15]([CH:2]([NH2:6])[C:1]([OH:5])=[O:4])=[CH:16][CH:17]=[C:12]([OH:18])[CH:13]=1Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
29.5 g of ammonium glyoxylate, 75 g of ammonium acetate, 60 g of phenol and 130 ml of water are treated in the same manner as described in Example 1. 21.9 g of DL-p-hydroxyphenylglycine are thereby obtained as crystals. Yield: 40.5%, M.p. 225°-228° C. (decomp.).
Quellen und Nachweise
- ORD-Eintrag
- ord-c605927454c2450b96b11c849caeabf7
- Quelldatensatz
- uspto-grants-1979_11
- Patentnummer
- US04175206
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