Iodoethane → HCID 66736185, Verbindung

HRID 470519Notizen

Reaktionsgleichung

[Br:1][C:2]1[CH:7]=[C:6]([CH3:8])[NH:5][C:4](=[O:9])[CH:3]=1.[CH2:10](I)[CH3:11].C([O-])([O-])=O.[K+].[K+]>>[Br:1][C:2]1[CH:7]=[C:6]([CH3:8])[N:5]([CH2:10][CH3:11])[C:4](=[O:9])[CH:3]=1

Komponenten

Edukt 3

HCID 6340Iodoethane

HCID 11430Potassium Carbonate

HCID 231494724-Bromo-6-methylpyridin-2-ol

Produkt 1

HCID 66736185HCID 66736185, Verbindung

Versuchsvorschrift

4-bromo-1-ethyl-6-methylpyridin-2(1H)-one was prepared by alkylation of 4-bromo-6-methylpyridin-2(1H)-one with ethyl iodide using K2CO3 following a procedure analogous to that described in Example 59 Step 1.

Quellen und Nachweise

ORD-Eintrag: ord-0936e0028a55411f9e61aecc88d267a8
Quelldatensatz: uspto-grants-2014_01
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08629138B2

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