Aminoacetaldehyde dimethyl acetal → HCID 44997787, Verbindung
Reaktionsgleichung
C([O:3][C:4](=O)[C:5]([NH:7][CH2:8][CH3:9])=[O:6])C.[CH3:11][O:12][CH:13]([O:16][CH3:17])[CH2:14][NH2:15]>CC(O)C>[CH3:11][O:12][CH:13]([O:16][CH3:17])[CH2:14][NH:15][C:4](=[O:3])[C:5]([NH:7][CH2:8][CH3:9])=[O:6]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
59.9 g (412.6 mM) of ethyl(ethylamino)(oxo)acetate and 45 ml (412.6 mM) of (2,2-dimethoxyethyl)amine in 480 ml of 2-propanol were stirred at room temperature for 16 h. A white precipitate was filtered, washed with 2-propanol and dried under vacuum, to give 67.8 g of N-(2,2-dimethoxyethyl)-N′-ethylethanediamide. Yield: 80.5%.
Aufarbeitung
- filtrationA white precipitate was filtered
- washwashed with 2-propanol
- customdried under vacuum
Quellen und Nachweise
- ORD-Eintrag
- ord-cc2d719fbc2a4c6b8aaa7e75bcf5bcbf
- Quelldatensatz
- uspto-grants-2014_01
- Patentnummer
- US08637522B2
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