Reaktionsgleichung
[CH:1]1([C:4](=[O:8])[CH2:5][C:6]#[N:7])[CH2:3][CH2:2]1.[CH2:9]([N:12]=[C:13]=[O:14])[CH:10]=[CH2:11]>>[CH2:9]([NH:12][C:13]([CH:5]([C:4]([CH:1]1[CH2:3][CH2:2]1)=[O:8])[C:6]#[N:7])=[O:14])[CH:10]=[CH2:11]Komponenten
3
Versuchsvorschrift
When β-cyclopropyl-β-oxopropionitrile (2,.00 g, 18.3 mmoles) [prepared in Example 1, Step A]was reacted with allylisocyanate (1.60 g, 19.2 mmoles) according to the general procedure of Example 1, Sep B, the title compound (2.8 g) was obtained as a white solid after recrystallization from 30% aqueous ethanol, m.p. 72°-73.5° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-0c2a43dc01f440d691a6f257f5a132a4
- Quelldatensatz
- uspto-grants-1989_12
- Patentnummer
- US04888357
Verknüpfte Notizen
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