Ammonium nitrate → Bentazone ammonium

HRID 482302

Reaktionsgleichung

Reaktionsgleichung von HRID 482302
[N+:1]([O-])([O-])=O.[NH4+].[CH3:6][CH:7]([N:9]1[S:19](=[O:21])(=[O:20])[N-:18][C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[C:10]1=[O:11])[CH3:8].[Na+]>O>[CH3:8][CH:7]([N:9]1[S:19](=[O:21])(=[O:20])[NH:18][C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[C:10]1=[O:11])[CH3:6].[NH4+:1]

Komponenten

4

Edukt 2

HCID 22985Ammonium nitrateHCID 13124860Bentazone-sodium

Produkt 1

HCID 131720800Bentazone ammoniumAusbeute 73,2 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Reaktionsbedingungen

Temperatur
20 °C

Versuchsvorschrift

8 g of ammonium nitrate were introduced at 50° C. with stirring into a solution of 26.3 g of bentazone-sodium in 21.7 g of water, and the reaction mixture was subsequently stirred for a further hour. After cooling to 20° C., the precipitate was filtered off, washed twice with 5 ml of ice water in each case and dried under reduced pressure and at 50° C. 18.9 g of bentazone-ammonium of 99% purity were obtained.

Aufarbeitung

  1. filtrationthe precipitate was filtered off
  2. washwashed twice with 5 ml of ice water in each case
  3. customdried under reduced pressure and at 50° C

Quellen und Nachweise

ORD-Eintrag
ord-7473581cb0484df3816afca8d4efcaec
Quelldatensatz
uspto-grants-1998_08
Patentnummer
US05795983

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