Hydrochloric Acid → HCID 20135785, Verbindung

HRID 484869Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 484869
[CH2:1]([N:3]([CH2:19][CH3:20])[CH2:4][CH2:5][CH2:6][NH:7][C:8]1[C:16]2[C:11](=[C:12]([NH2:18])[CH:13]=[C:14]([NH2:17])[CH:15]=2)[NH:10][N:9]=1)[CH3:2].[ClH:21].C(OCC)C>C(O)C>[ClH:21].[ClH:21].[ClH:21].[CH2:19]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][CH2:6][NH:7][C:8]1[C:16]2[C:11](=[C:12]([NH2:18])[CH:13]=[C:14]([NH2:17])[CH:15]=2)[NH:10][N:9]=1)[CH3:20]

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 20135762HCID 20135762, Verbindung

Produkt 1

HCID 20135785HCID 20135785, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

In 20 ml of absolute ethyl alcohol was dissolved 2.0 g of the 3-(3-diethylaminopropylamino)-5,7-diaminoindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 3-(3-diethylaminopropylamino)-5,7-diaminoindazole trihydrochloride having the following analytical value.

Aufarbeitung

  1. temperatureunder cooling with ice
  2. customto separate crystals
  3. customThe crystals were obtained by filtration
  4. customdried

Quellen und Nachweise

ORD-Eintrag
ord-e1dc755c67e64350ba532780a7812372
Quelldatensatz
uspto-grants-1985_08
Patentnummer
US04533731

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