Hydrochloric Acid → HCID 20135842, Verbindung

HRID 484910Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 484910
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[NH:13][N:12]=2)[CH2:3][CH2:2]1.[ClH:20].C(OCC)C>C(O)C>[ClH:20].[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[NH:13][N:12]=2)[CH2:3][CH2:2]1

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 3065651Indazole, 3-((3-morpholinopropyl)amino)-

Produkt 1

HCID 20135842HCID 20135842, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

In 15 ml of absolute ethyl alcohol was dissolved 1.0 g of the 3-(3-morpholinopropylamino)indazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 3-(3-morpholinopropylamino)indazole hydrochloride having the following analytical value.

Aufarbeitung

  1. temperatureunder cooling with ice
  2. customto separate crystals
  3. customThe crystals were obtained by filtration
  4. customdried

Quellen und Nachweise

ORD-Eintrag
ord-d25f2f454ce7457fb7b1120fe2204575
Quelldatensatz
uspto-grants-1985_08
Patentnummer
US04533731

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