Methyl 2-(1-methylpiperidin-4-ylidene)acetate → Methyl 2-(1-methylpiperidin-4-yl)acetate

HRID 495482Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 495482
[CH3:1][O:2][C:3](=[O:12])[CH:4]=[C:5]1[CH2:10][CH2:9][N:8]([CH3:11])[CH2:7][CH2:6]1>[Pd].CCO>[CH3:1][O:2][C:3](=[O:12])[CH2:4][CH:5]1[CH2:6][CH2:7][N:8]([CH3:11])[CH2:9][CH2:10]1

Komponenten

4

Edukt 1

HCID 20672702Methyl 2-(1-methylpiperidin-4-ylidene)acetate

Produkt 1

HCID 19425952Methyl 2-(1-methylpiperidin-4-yl)acetate

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 23938PalladiumKatalysatorHCID 702EthanolLösungsmittel

Versuchsvorschrift

(1-Methyl-piperidin-4-ylidene)-acetic acid methyl ester (Step A) was stirred under H2 overnight (1.1 g of 10% Pd/C and 200 mL EtOH), filtered and evaporated to give (1-methyl-piperidin-4-yl)-acetic acid methyl ester as a yellow oil/white solid.

Aufarbeitung

  1. filtrationfiltered
  2. customevaporated

Quellen und Nachweise

ORD-Eintrag
ord-dacca3ed436b4d0f94be5b29df70d83f
Quelldatensatz
uspto-grants-2005_09
Patentnummer
US06939874B2

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